Crystallography Open Database

Information card for entry 7061676

Preview

Coordinates	7061676.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C14 H36 O3.5 P2 Rh Si
Calculated formula	C14 H36 O3.5 P2 Rh Si
Title of publication	Multinuclear rhodium complexes supported by tetra-tert-butoxy disiloxide ligand: synthesis, structure, and reactivity
Authors of publication	Ishizaka, Yusuke; Matsumoto, Kazuhiro; Sato, Kazuhiko; Choi, Jun-Chul
Journal of publication	New Journal of Chemistry
Year of publication	2022
Journal volume	46
Journal issue	33
Pages of publication	16040 - 16046
a	18.8299 ± 0.0003 Å
b	11.579 ± 0.0002 Å
c	20.3542 ± 0.0004 Å
α	90°
β	102.325 ± 0.002°
γ	90°
Cell volume	4335.57 ± 0.14 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	I 1 2/a 1
Hall space group symbol	-I 2ya
Residual factor for all reflections	0.0162
Residual factor for significantly intense reflections	0.0155
Weighted residual factors for significantly intense reflections	0.0381
Weighted residual factors for all reflections included in the refinement	0.0384
Goodness-of-fit parameter for all reflections included in the refinement	1.09
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
277671 (current)	2022-09-06	cif/ Updating files of 7061675, 7061676, 7061677 Original log message: Adding full bibliography for 7061675--7061677.cif.	7061676.cif
276953	2022-07-27	cif/ Adding structures of 7061675, 7061676, 7061677 via cif-deposit CGI script.	7061676.cif