Crystallography Open Database

Information card for entry 7113817

Preview

Coordinates	7113817.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C176 H112 Ag6 Br8 F12 N8 O12 P10 Re4
Calculated formula	C176 H112 Ag6 Br8 F12 N8 O12 P10 Re4
Title of publication	Synthesis and luminescence behaviour of novel heterodecanuclear silver(I)–rhenium(I) alkynyl complexes. X-Ray crystal structures of [Ag6(μ-dppm)4{μ3-C≡CC≡C–Re(Me2bpy)(CO)3}4](PF6)2 and [Ag6(μ-dppm)4{μ3-C≡CC≡C–Re(Br2phen)(CO)3}4](PF6)2
Authors of publication	Yam, Vivian Wing-Wah; Lo, Wing-Yin; Zhu, Nianyong
Journal of publication	Chemical Communications (Cambridge, United Kingdom)
Year of publication	2003
Journal issue	19
Pages of publication	2446 - 2447
a	27.379 ± 0.004 Å
b	27.379 ± 0.004 Å
c	16.984 ± 0.003 Å
α	90°
β	90°
γ	90°
Cell volume	12731 ± 3 Å³
Cell temperature	253 ± 2 K
Ambient diffraction temperature	253 ± 2 K
Number of distinct elements	9
Space group number	86
Hermann-Mauguin space group symbol	P 42/n :2
Hall space group symbol	-P 4bc
Residual factor for all reflections	0.1023
Residual factor for significantly intense reflections	0.0665
Weighted residual factors for significantly intense reflections	0.2207
Weighted residual factors for all reflections included in the refinement	0.2395
Goodness-of-fit parameter for all reflections included in the refinement	1.019
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
297215 (current)	2025-01-08	Updated bibliography in entries 7113816-7113817.	7113817.cif
180252	2016-03-26	cif/7/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/11/38.	7113817.cif
115289	2014-06-02	cif/ Adding structures of 7113816, 7113817 via cif-deposit CGI script.	7113817.cif