Crystallography Open Database

Information card for entry 7121396

Preview

Coordinates	7121396.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C21 H4 O18 Os6
Calculated formula	C21 H4 O18 Os6
Title of publication	Multiple cluster CH activations and transformations of furan by triosmium carbonyl complexes.
Authors of publication	Adams, Richard D.; Kiprotich, Emmanuel J.; Smith, Mark D.
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2018
Journal volume	54
Journal issue	28
Pages of publication	3464 - 3467
a	9.4304 ± 0.0005 Å
b	9.4911 ± 0.0005 Å
c	20.117 ± 0.0009 Å
α	98.507 ± 0.002°
β	95.159 ± 0.002°
γ	119.294 ± 0.001°
Cell volume	1525.29 ± 0.14 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0501
Residual factor for significantly intense reflections	0.0306
Weighted residual factors for significantly intense reflections	0.0434
Weighted residual factors for all reflections included in the refinement	0.0474
Goodness-of-fit parameter for all reflections included in the refinement	1.081
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
227980 (current)	2019-11-17	cif/ Updating files of 7121393, 7121394, 7121395, 7121396, 7121397, 7121398 Original log message: Adding full bibliography for 7121393--7121398.cif.	7121396.cif
206938	2018-03-14	cif/ Adding structures of 7121393, 7121394, 7121395, 7121396, 7121397, 7121398 via cif-deposit CGI script.	7121396.cif