Crystallography Open Database

Information card for entry 7121397

Preview

Coordinates	7121397.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C23 H4 O20 Os6
Calculated formula	C23 H4 O20 Os6
Title of publication	Multiple cluster CH activations and transformations of furan by triosmium carbonyl complexes.
Authors of publication	Adams, Richard D.; Kiprotich, Emmanuel J.; Smith, Mark D.
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2018
Journal volume	54
Journal issue	28
Pages of publication	3464 - 3467
a	14.026 ± 0.0007 Å
b	9.5121 ± 0.0005 Å
c	24.6707 ± 0.0013 Å
α	90°
β	96.081 ± 0.002°
γ	90°
Cell volume	3273 ± 0.3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.044
Residual factor for significantly intense reflections	0.0291
Weighted residual factors for significantly intense reflections	0.0512
Weighted residual factors for all reflections included in the refinement	0.0551
Goodness-of-fit parameter for all reflections included in the refinement	1.059
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
227980 (current)	2019-11-17	cif/ Updating files of 7121393, 7121394, 7121395, 7121396, 7121397, 7121398 Original log message: Adding full bibliography for 7121393--7121398.cif.	7121397.cif
206938	2018-03-14	cif/ Adding structures of 7121393, 7121394, 7121395, 7121396, 7121397, 7121398 via cif-deposit CGI script.	7121397.cif