Crystallography Open Database

Information card for entry 7121398

Preview

Coordinates	7121398.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H4 O19 Os6
Calculated formula	C22 H4 O19 Os6
Title of publication	Multiple cluster CH activations and transformations of furan by triosmium carbonyl complexes.
Authors of publication	Adams, Richard D.; Kiprotich, Emmanuel J.; Smith, Mark D.
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2018
Journal volume	54
Journal issue	28
Pages of publication	3464 - 3467
a	9.7044 ± 0.0005 Å
b	11.2944 ± 0.0005 Å
c	15.7359 ± 0.0007 Å
α	82.9237 ± 0.0016°
β	86.2639 ± 0.0016°
γ	67.6042 ± 0.0015°
Cell volume	1582.19 ± 0.13 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0444
Residual factor for significantly intense reflections	0.0294
Weighted residual factors for significantly intense reflections	0.0467
Weighted residual factors for all reflections included in the refinement	0.0506
Goodness-of-fit parameter for all reflections included in the refinement	1.066
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
227980 (current)	2019-11-17	cif/ Updating files of 7121393, 7121394, 7121395, 7121396, 7121397, 7121398 Original log message: Adding full bibliography for 7121393--7121398.cif.	7121398.cif
206938	2018-03-14	cif/ Adding structures of 7121393, 7121394, 7121395, 7121396, 7121397, 7121398 via cif-deposit CGI script.	7121398.cif