Crystallography Open Database

Information card for entry 7121442

Preview

Coordinates	7121442.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H33 F8 Ge N7 O6 S2
Calculated formula	C32 H31 F8 Ge N7 O6 S2
Title of publication	Oxidation of a germanium(ii) dication to access cationic germanium(iv) fluorides.
Authors of publication	Suter, Riccardo; Swidan, Ala'aeddeen; Macdonald, Charles L. B.; Burford, Neil
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2018
Journal volume	54
Journal issue	33
Pages of publication	4140 - 4143
a	14.2065 ± 0.0006 Å
b	18.0706 ± 0.0008 Å
c	14.8299 ± 0.0008 Å
α	90°
β	106.697 ± 0.002°
γ	90°
Cell volume	3646.6 ± 0.3 Å³
Cell temperature	170 K
Ambient diffraction temperature	170 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0688
Residual factor for significantly intense reflections	0.0422
Weighted residual factors for significantly intense reflections	0.0954
Weighted residual factors for all reflections included in the refinement	0.1097
Goodness-of-fit parameter for all reflections included in the refinement	1.107
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
228119 (current)	2019-11-17	cif/ Updating files of 7121441, 7121442, 7121443 Original log message: Adding full bibliography for 7121441--7121443.cif.	7121442.cif
207115	2018-03-27	cif/ Adding structures of 7121441, 7121442, 7121443 via cif-deposit CGI script.	7121442.cif