Crystallography Open Database

Information card for entry 7121443

Preview

Coordinates	7121443.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H33 F6 Ge N7 O6 S2
Calculated formula	C32 H33 F6 Ge N7 O6 S2
Title of publication	Oxidation of a germanium(ii) dication to access cationic germanium(iv) fluorides.
Authors of publication	Suter, Riccardo; Swidan, Ala'aeddeen; Macdonald, Charles L. B.; Burford, Neil
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2018
Journal volume	54
Journal issue	33
Pages of publication	4140 - 4143
a	14.7605 ± 0.0007 Å
b	11.2818 ± 0.0005 Å
c	21.5537 ± 0.001 Å
α	90°
β	96.184 ± 0.002°
γ	90°
Cell volume	3568.3 ± 0.3 Å³
Cell temperature	150 K
Ambient diffraction temperature	150 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.043
Residual factor for significantly intense reflections	0.032
Weighted residual factors for significantly intense reflections	0.0798
Weighted residual factors for all reflections included in the refinement	0.0864
Goodness-of-fit parameter for all reflections included in the refinement	1.0506
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
228119 (current)	2019-11-17	cif/ Updating files of 7121441, 7121442, 7121443 Original log message: Adding full bibliography for 7121441--7121443.cif.	7121443.cif
207115	2018-03-27	cif/ Adding structures of 7121441, 7121442, 7121443 via cif-deposit CGI script.	7121443.cif