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Information card for entry 7122767
Preview
| Coordinates | 7122767.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C31 H38 O Si2 |
|---|---|
| Calculated formula | C31 H38 O Si2 |
| Title of publication | Synthesis of carbonyl-bridged dibenzofulvalenes and related compounds by rhodium-catalyzed stitching reaction. |
| Authors of publication | Shintani, Ryo; Kishikawa, Shinnosuke; Nakamura, Kimihiro; Tsuda, Tomohiro; Nozaki, Kyoko |
| Journal of publication | Chemical communications (Cambridge, England) |
| Year of publication | 2019 |
| a | 10.441 ± 0.006 Å |
| b | 11.776 ± 0.006 Å |
| c | 12.121 ± 0.007 Å |
| α | 76.44 ± 0.02° |
| β | 80.25 ± 0.02° |
| γ | 76.74 ± 0.02° |
| Cell volume | 1399.6 ± 1.4 Å3 |
| Cell temperature | 93 K |
| Ambient diffraction temperature | 93 K |
| Number of distinct elements | 4 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.1535 |
| Residual factor for significantly intense reflections | 0.0966 |
| Weighted residual factors for significantly intense reflections | 0.1618 |
| Weighted residual factors for all reflections included in the refinement | 0.1881 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.08 |
| Diffraction radiation wavelength | 0.71075 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 212895 (current) | 2019-01-11 | cif/ Adding structures of 7122767, 7122768, 7122769, 7122770 via cif-deposit CGI script. |
7122767.cif |
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Users of the data should acknowledge the original authors of the
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