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Information card for entry 7122768
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| Coordinates | 7122768.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Chemical name | Ge |
|---|---|
| Formula | C26 H28 Ge |
| Calculated formula | C26 H28 Ge |
| Title of publication | Synthesis of carbonyl-bridged dibenzofulvalenes and related compounds by rhodium-catalyzed stitching reaction. |
| Authors of publication | Shintani, Ryo; Kishikawa, Shinnosuke; Nakamura, Kimihiro; Tsuda, Tomohiro; Nozaki, Kyoko |
| Journal of publication | Chemical communications (Cambridge, England) |
| Year of publication | 2019 |
| a | 16.8701 ± 0.0006 Å |
| b | 16.9405 ± 0.0006 Å |
| c | 18.3624 ± 0.0003 Å |
| α | 100.752 ± 0.002° |
| β | 100.803 ± 0.002° |
| γ | 119.398 ± 0.004° |
| Cell volume | 4246.4 ± 0.3 Å3 |
| Cell temperature | 113 K |
| Ambient diffraction temperature | 113 K |
| Number of distinct elements | 3 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0445 |
| Residual factor for significantly intense reflections | 0.0297 |
| Weighted residual factors for significantly intense reflections | 0.063 |
| Weighted residual factors for all reflections included in the refinement | 0.0648 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.979 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 212895 (current) | 2019-01-11 | cif/ Adding structures of 7122767, 7122768, 7122769, 7122770 via cif-deposit CGI script. |
7122768.cif |
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Users of the data should acknowledge the original authors of the
structural data.