Crystallography Open Database

Information card for entry 7124908

Preview

Coordinates	7124908.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C33 H53 B Br N3 O Si Zn
Calculated formula	C33 H53 B Br N3 O Si Zn
Title of publication	Two-coordinate terminal zinc hydride complexes: synthesis, structure and preliminary reactivity studies.
Authors of publication	Dawkins, Michael J. C.; Middleton, Ewart; Kefalidis, Christos E.; Dange, Deepak; Juckel, Martin M.; Maron, Laurent; Jones, Cameron
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2016
Journal volume	52
Journal issue	69
Pages of publication	10490 - 10492
a	15.203 ± 0.003 Å
b	11.974 ± 0.002 Å
c	19.965 ± 0.004 Å
α	90°
β	100.3 ± 0.03°
γ	90°
Cell volume	3575.9 ± 1.2 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	8
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0516
Residual factor for significantly intense reflections	0.0327
Weighted residual factors for significantly intense reflections	0.0676
Weighted residual factors for all reflections included in the refinement	0.0739
Goodness-of-fit parameter for all reflections included in the refinement	1.009
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
234338 (current)	2019-11-23	cif/ Adding structures of 7124906, 7124907, 7124908, 7124909, 7124910, 7124911, 7124912, 7124913, 7124914 via cif-deposit CGI script.	7124908.cif