Crystallography Open Database

Information card for entry 7124909

Preview

Coordinates	7124909.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C84 H98 N2 O2 Si2 Zn2
Calculated formula	C84 H98 N2 O2 Si2 Zn2
Title of publication	Two-coordinate terminal zinc hydride complexes: synthesis, structure and preliminary reactivity studies.
Authors of publication	Dawkins, Michael J. C.; Middleton, Ewart; Kefalidis, Christos E.; Dange, Deepak; Juckel, Martin M.; Maron, Laurent; Jones, Cameron
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2016
Journal volume	52
Journal issue	69
Pages of publication	10490 - 10492
a	13.39 ± 0.003 Å
b	14.317 ± 0.003 Å
c	20.067 ± 0.004 Å
α	80.79 ± 0.03°
β	79.66 ± 0.03°
γ	71.54 ± 0.03°
Cell volume	3567.7 ± 1.5 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0426
Residual factor for significantly intense reflections	0.0385
Weighted residual factors for significantly intense reflections	0.0998
Weighted residual factors for all reflections included in the refinement	0.1023
Goodness-of-fit parameter for all reflections included in the refinement	1.047
Diffraction radiation wavelength	0.7109 Å
Diffraction radiation type	Synchrotron
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
234338 (current)	2019-11-23	cif/ Adding structures of 7124906, 7124907, 7124908, 7124909, 7124910, 7124911, 7124912, 7124913, 7124914 via cif-deposit CGI script.	7124909.cif