Crystallography Open Database

Information card for entry 7232934

Preview

Coordinates	7232934.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C33 H16 Mn2 N17 O6 W
Calculated formula	C33 H16 Mn2 N17 O6 W
Title of publication	In situ formed [M(CN)9] (M = W, Mo) as a building block for the construction of two nona-cyanometalate-bridged heterometallic coordination polymers
Authors of publication	Qian, Jun; Yoshikawa, Hirofumi; Humphrey, Mark G.; Zhang, Jinfang; Awaga, Kunio; Zhang, Chi
Journal of publication	CrystEngComm
Year of publication	2019
Journal volume	21
Journal issue	29
Pages of publication	4363
a	14.47 ± 0.002 Å
b	14.47 ± 0.002 Å
c	28.017 ± 0.006 Å
α	90°
β	90°
γ	90°
Cell volume	5866.2 ± 1.7 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	87
Hermann-Mauguin space group symbol	I 4/m
Hall space group symbol	-I 4
Residual factor for all reflections	0.0551
Residual factor for significantly intense reflections	0.0517
Weighted residual factors for significantly intense reflections	0.1438
Weighted residual factors for all reflections included in the refinement	0.1459
Goodness-of-fit parameter for all reflections included in the refinement	1.245
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
223472 (current)	2019-11-07	cif/ Updating files of 7232934, 7232935 Original log message: Adding full bibliography for 7232934--7232935.cif.	7232934.cif
216541	2019-06-26	cif/ Adding structures of 7232934, 7232935 via cif-deposit CGI script.	7232934.cif