Crystallography Open Database

Information card for entry 7232935

Preview

Coordinates	7232935.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C45 H44 Mn2 Mo N21 O10
Calculated formula	C45 H44 Mn2 Mo N21 O10
Title of publication	In situ formed [M(CN)9] (M = W, Mo) as a building block for the construction of two nona-cyanometalate-bridged heterometallic coordination polymers
Authors of publication	Qian, Jun; Yoshikawa, Hirofumi; Humphrey, Mark G.; Zhang, Jinfang; Awaga, Kunio; Zhang, Chi
Journal of publication	CrystEngComm
Year of publication	2019
Journal volume	21
Journal issue	29
Pages of publication	4363
a	14.45 ± 0.002 Å
b	14.45 ± 0.002 Å
c	28.044 ± 0.006 Å
α	90°
β	90°
γ	90°
Cell volume	5855.7 ± 1.7 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	87
Hermann-Mauguin space group symbol	I 4/m
Hall space group symbol	-I 4
Residual factor for all reflections	0.0681
Residual factor for significantly intense reflections	0.0644
Weighted residual factors for significantly intense reflections	0.184
Weighted residual factors for all reflections included in the refinement	0.1879
Goodness-of-fit parameter for all reflections included in the refinement	1.098
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
223472 (current)	2019-11-07	cif/ Updating files of 7232934, 7232935 Original log message: Adding full bibliography for 7232934--7232935.cif.	7232935.cif
216541	2019-06-26	cif/ Adding structures of 7232934, 7232935 via cif-deposit CGI script.	7232935.cif