Crystallography Open Database

Information card for entry 7243735

Preview

Coordinates	7243735.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C12 H14 N14 O6 Pb2 S2
Calculated formula	C12 H14 N14 O6 Pb2 S2
Title of publication	Lead(ii) supramolecular structures formed through a cooperative influence of the hydrazinecarbothioamide derived and ancillary ligands
Authors of publication	García-Santos, Isabel; Castiñeiras, Alfonso; Mahmoudi, Ghodrat; Babashkina, Maria G.; Zangrando, Ennio; Gomila, Rosa M.; Frontera, Antonio; Safin, Damir A.
Journal of publication	CrystEngComm
Year of publication	2022
Journal volume	24
Journal issue	2
Pages of publication	368 - 378
a	7.1834 ± 0.0008 Å
b	7.7618 ± 0.0008 Å
c	10.873 ± 0.0012 Å
α	89.66 ± 0.004°
β	76.812 ± 0.004°
γ	71.301 ± 0.003°
Cell volume	557.61 ± 0.11 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0172
Residual factor for significantly intense reflections	0.0144
Weighted residual factors for significantly intense reflections	0.028
Weighted residual factors for all reflections included in the refinement	0.0289
Goodness-of-fit parameter for all reflections included in the refinement	1.099
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
272624 (current)	2022-02-04	cif/ Updating files of 7243734, 7243735, 7243736, 7243737 Original log message: Adding full bibliography for 7243734--7243737.cif.	7243735.cif
269925	2021-10-14	cif/ Adding structures of 7243734, 7243735, 7243736, 7243737 via cif-deposit CGI script.	7243735.cif