Crystallography Open Database

Information card for entry 7243736

Preview

Coordinates	7243736.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18 H22 N12 O Pb2 S4
Calculated formula	C18 H22 N12 O Pb2 S4
Title of publication	Lead(ii) supramolecular structures formed through a cooperative influence of the hydrazinecarbothioamide derived and ancillary ligands
Authors of publication	García-Santos, Isabel; Castiñeiras, Alfonso; Mahmoudi, Ghodrat; Babashkina, Maria G.; Zangrando, Ennio; Gomila, Rosa M.; Frontera, Antonio; Safin, Damir A.
Journal of publication	CrystEngComm
Year of publication	2022
Journal volume	24
Journal issue	2
Pages of publication	368 - 378
a	20.419 ± 0.001 Å
b	10.2159 ± 0.0006 Å
c	12.8155 ± 0.0007 Å
α	90°
β	99.731 ± 0.002°
γ	90°
Cell volume	2634.8 ± 0.2 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0248
Residual factor for significantly intense reflections	0.0186
Weighted residual factors for significantly intense reflections	0.034
Weighted residual factors for all reflections included in the refinement	0.0353
Goodness-of-fit parameter for all reflections included in the refinement	1.057
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
272624 (current)	2022-02-04	cif/ Updating files of 7243734, 7243735, 7243736, 7243737 Original log message: Adding full bibliography for 7243734--7243737.cif.	7243736.cif
269925	2021-10-14	cif/ Adding structures of 7243734, 7243735, 7243736, 7243737 via cif-deposit CGI script.	7243736.cif