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Information card for entry 7244562
Preview
| Coordinates | 7244562.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | bis(p-Miranphos)palladium(II) dichloride |
|---|---|
| Formula | C45 H32 Cl2 F12 O5 P2 Pd |
| Calculated formula | C45 H32 Cl2 F12 O5 P2 Pd |
| Title of publication | Preparation of carboxylic arylphosphines by hydrolysis of the trifluoromethyl group |
| Authors of publication | Herrera, Daniel; Peral, Daniel; Bayón, J. Carles |
| Journal of publication | RSC Advances |
| Year of publication | 2022 |
| Journal volume | 12 |
| Journal issue | 12 |
| Pages of publication | 7103 - 7114 |
| a | 15.3938 ± 0.0007 Å |
| b | 15.6175 ± 0.0008 Å |
| c | 20.4211 ± 0.001 Å |
| α | 90° |
| β | 97.107 ± 0.001° |
| γ | 90° |
| Cell volume | 4871.8 ± 0.4 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0709 |
| Residual factor for significantly intense reflections | 0.0475 |
| Weighted residual factors for significantly intense reflections | 0.1158 |
| Weighted residual factors for all reflections included in the refinement | 0.1288 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.029 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 273218 (current) | 2022-03-03 | cif/ Adding structures of 7244562, 7244563 via cif-deposit CGI script. |
7244562.cif |
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Users of the data should acknowledge the original authors of the
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