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Information card for entry 7244563
Preview
| Coordinates | 7244563.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C42 H26 Cl2 F12 O4 P2 Pd |
|---|---|
| Calculated formula | C42 H26 Cl2 F12 O4 P2 Pd |
| Title of publication | Preparation of carboxylic arylphosphines by hydrolysis of the trifluoromethyl group |
| Authors of publication | Herrera, Daniel; Peral, Daniel; Bayón, J. Carles |
| Journal of publication | RSC Advances |
| Year of publication | 2022 |
| Journal volume | 12 |
| Journal issue | 12 |
| Pages of publication | 7103 - 7114 |
| a | 10.1026 ± 0.0005 Å |
| b | 27.1594 ± 0.0013 Å |
| c | 36.7299 ± 0.0017 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 10078 ± 0.8 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 61 |
| Hermann-Mauguin space group symbol | P b c a |
| Hall space group symbol | -P 2ac 2ab |
| Residual factor for all reflections | 0.1889 |
| Residual factor for significantly intense reflections | 0.0832 |
| Weighted residual factors for significantly intense reflections | 0.2291 |
| Weighted residual factors for all reflections included in the refinement | 0.2908 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.028 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 273218 (current) | 2022-03-03 | cif/ Adding structures of 7244562, 7244563 via cif-deposit CGI script. |
7244563.cif |
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Users of the data should acknowledge the original authors of the
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