Crystallography Open Database

Information card for entry 7246045

Preview

Coordinates	7246045.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C46 H56 Dy5 N3 O24
Calculated formula	C46 H59 Dy5 N3 O24
Title of publication	Synthesis, structures and magnetic properties of four dysprosium-based complexes with a multidentate ligand with steric constraint
Authors of publication	Li, Wen-Qiang; Ma, Meng-Xia; Ni, Qing-Ling; Li, Shi-Ming; Gui, Liu-Cheng; Wang, Xiu-Jian
Journal of publication	CrystEngComm
Year of publication	2023
Journal volume	25
Journal issue	4
Pages of publication	614 - 621
a	10.9825 ± 0.0001 Å
b	22.9575 ± 0.0002 Å
c	23.0079 ± 0.0002 Å
α	90°
β	98.137 ± 0.001°
γ	90°
Cell volume	5742.6 ± 0.09 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100.15 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0534
Residual factor for significantly intense reflections	0.0486
Weighted residual factors for significantly intense reflections	0.1218
Weighted residual factors for all reflections included in the refinement	0.1244
Goodness-of-fit parameter for all reflections included in the refinement	1.111
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
281430 (current)	2023-03-04	cif/ Updating files of 7246045, 7246046, 7246047, 7246048 Original log message: Adding full bibliography for 7246045--7246048.cif.	7246045.cif
280022	2022-12-24	cif/ Adding structures of 7246045, 7246046, 7246047, 7246048 via cif-deposit CGI script.	7246045.cif