Crystallography Open Database

Information card for entry 7246046

Preview

Coordinates	7246046.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C60 H60 Cl6 Dy4 N6 O14
Calculated formula	C60 H64 Cl6 Dy4 N6 O14
Title of publication	Synthesis, structures and magnetic properties of four dysprosium-based complexes with a multidentate ligand with steric constraint
Authors of publication	Li, Wen-Qiang; Ma, Meng-Xia; Ni, Qing-Ling; Li, Shi-Ming; Gui, Liu-Cheng; Wang, Xiu-Jian
Journal of publication	CrystEngComm
Year of publication	2023
Journal volume	25
Journal issue	4
Pages of publication	614 - 621
a	10.925 ± 0.0003 Å
b	11.2522 ± 0.0004 Å
c	16.2537 ± 0.0005 Å
α	96.322 ± 0.003°
β	98.838 ± 0.002°
γ	111.745 ± 0.003°
Cell volume	1803.23 ± 0.11 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0425
Residual factor for significantly intense reflections	0.0293
Weighted residual factors for significantly intense reflections	0.0597
Weighted residual factors for all reflections included in the refinement	0.0658
Goodness-of-fit parameter for all reflections included in the refinement	1.045
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
281430 (current)	2023-03-04	cif/ Updating files of 7246045, 7246046, 7246047, 7246048 Original log message: Adding full bibliography for 7246045--7246048.cif.	7246046.cif
280022	2022-12-24	cif/ Adding structures of 7246045, 7246046, 7246047, 7246048 via cif-deposit CGI script.	7246046.cif