Crystallography Open Database

Information card for entry 7700249

Preview

Coordinates	7700249.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C14 H33 Li N2 Si
Calculated formula	C14 H33 Li N2 Si
Title of publication	The smaller, the better? How the aggregate size affects the reactivity of (trimethylsilyl)methyllithium.
Authors of publication	Knauer, Lena; Wattenberg, Jonathan; Kroesen, Ulrike; Strohmann, Carsten
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	30
Pages of publication	11285 - 11291
a	7.4127 ± 0.0003 Å
b	12.3217 ± 0.0005 Å
c	10.0582 ± 0.0004 Å
α	90°
β	105.694 ± 0.002°
γ	90°
Cell volume	884.44 ± 0.06 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	5
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0345
Residual factor for significantly intense reflections	0.0334
Weighted residual factors for significantly intense reflections	0.0885
Weighted residual factors for all reflections included in the refinement	0.0898
Goodness-of-fit parameter for all reflections included in the refinement	1.047
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
224341 (current)	2019-11-08	cif/ Updating files of 7700249, 7700250, 7700251 Original log message: Adding full bibliography for 7700249--7700251.cif.	7700249.cif
215906	2019-06-13	cif/ Adding structures of 7700249, 7700250, 7700251 via cif-deposit CGI script.	7700249.cif