Crystallography Open Database

Information card for entry 7700281

Preview

Coordinates	7700281.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C20 H41 Cl4 N P2 Si4
Calculated formula	C20 H41 Cl4 N P2 Si4
Title of publication	[E(μ-NBbp)]<sub>2</sub> (E = P, As) - group 15 biradicals synthesized from acyclic precursors.
Authors of publication	Bresien, Jonas; Schulz, Axel; Szych, Lilian Sophie; Villinger, Alexander; Wustrack, Ronald
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	29
Pages of publication	11103 - 11111
a	20.7415 ± 0.0007 Å
b	17.8599 ± 0.0007 Å
c	17.9973 ± 0.0006 Å
α	90°
β	107.625 ± 0.001°
γ	90°
Cell volume	6354 ± 0.4 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0874
Residual factor for significantly intense reflections	0.0408
Weighted residual factors for significantly intense reflections	0.077
Weighted residual factors for all reflections included in the refinement	0.0942
Goodness-of-fit parameter for all reflections included in the refinement	1.019
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
223760 (current)	2019-11-07	cif/ Updating files of 7700277, 7700278, 7700279, 7700280, 7700281, 7700282, 7700283 Original log message: Adding full bibliography for 7700277--7700283.cif.	7700281.cif
216039	2019-06-18	cif/ Adding structures of 7700277, 7700278, 7700279, 7700280, 7700281, 7700282, 7700283 via cif-deposit CGI script.	7700281.cif