Crystallography Open Database

Information card for entry 7700282

Preview

Coordinates	7700282.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C20 H42 Cl2 N P Si4
Calculated formula	C20 H42 Cl2 N P Si4
Title of publication	[E(μ-NBbp)]<sub>2</sub> (E = P, As) - group 15 biradicals synthesized from acyclic precursors.
Authors of publication	Bresien, Jonas; Schulz, Axel; Szych, Lilian Sophie; Villinger, Alexander; Wustrack, Ronald
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	29
Pages of publication	11103 - 11111
a	13.9382 ± 0.0008 Å
b	12.557 ± 0.0005 Å
c	33.8982 ± 0.0014 Å
α	90°
β	90°
γ	90°
Cell volume	5932.9 ± 0.5 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	6
Space group number	61
Hermann-Mauguin space group symbol	P b c a
Hall space group symbol	-P 2ac 2ab
Residual factor for all reflections	0.0993
Residual factor for significantly intense reflections	0.0747
Weighted residual factors for significantly intense reflections	0.1454
Weighted residual factors for all reflections included in the refinement	0.1549
Goodness-of-fit parameter for all reflections included in the refinement	1.15
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
223760 (current)	2019-11-07	cif/ Updating files of 7700277, 7700278, 7700279, 7700280, 7700281, 7700282, 7700283 Original log message: Adding full bibliography for 7700277--7700283.cif.	7700282.cif
216039	2019-06-18	cif/ Adding structures of 7700277, 7700278, 7700279, 7700280, 7700281, 7700282, 7700283 via cif-deposit CGI script.	7700282.cif