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Information card for entry 7701522
Preview
| Coordinates | 7701522.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C46 H60 N2 Ni O4 |
|---|---|
| Calculated formula | C46 H60 N2 Ni O4 |
| Title of publication | Novel dioxolene nickel complexes with sterically hindered diazabutadienes. Coupling of aza-ligands coordinated to nickel. |
| Authors of publication | Bubnov, Michael P.; Cherkasov, Vladimir K.; Teplova, Irina A.; Druzhkov, Nickolay O.; Grishin, Ivan D.; Baranov, Evgenii V.; Bogomyakov, Artem S.; Abakumov, Gleb A. |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2019 |
| Journal volume | 48 |
| Journal issue | 28 |
| Pages of publication | 10516 - 10525 |
| a | 9.9531 ± 0.0005 Å |
| b | 10.9403 ± 0.0006 Å |
| c | 19.9308 ± 0.0011 Å |
| α | 90.413 ± 0.001° |
| β | 101.939 ± 0.001° |
| γ | 95.382 ± 0.001° |
| Cell volume | 2113.2 ± 0.2 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0504 |
| Residual factor for significantly intense reflections | 0.0362 |
| Weighted residual factors for significantly intense reflections | 0.0872 |
| Weighted residual factors for all reflections included in the refinement | 0.0912 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.031 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 223295 (current) | 2019-11-05 | cif/ Adding structures of 7701522, 7701523, 7701524, 7701525 via cif-deposit CGI script. |
7701522.cif |
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Users of the data should acknowledge the original authors of the
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