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Information card for entry 7701523
Preview
| Coordinates | 7701523.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C52 H72 N2 Ni O4 |
|---|---|
| Calculated formula | C52 H72 N2 Ni O4 |
| Title of publication | Novel dioxolene nickel complexes with sterically hindered diazabutadienes. Coupling of aza-ligands coordinated to nickel. |
| Authors of publication | Bubnov, Michael P.; Cherkasov, Vladimir K.; Teplova, Irina A.; Druzhkov, Nickolay O.; Grishin, Ivan D.; Baranov, Evgenii V.; Bogomyakov, Artem S.; Abakumov, Gleb A. |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2019 |
| Journal volume | 48 |
| Journal issue | 28 |
| Pages of publication | 10516 - 10525 |
| a | 16.2618 ± 0.0003 Å |
| b | 16.2618 ± 0.0003 Å |
| c | 35.9463 ± 0.0016 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 9505.9 ± 0.5 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 88 |
| Hermann-Mauguin space group symbol | I 41/a :2 |
| Hall space group symbol | -I 4ad |
| Residual factor for all reflections | 0.0417 |
| Residual factor for significantly intense reflections | 0.0336 |
| Weighted residual factors for significantly intense reflections | 0.0815 |
| Weighted residual factors for all reflections included in the refinement | 0.0863 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.01 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 223295 (current) | 2019-11-05 | cif/ Adding structures of 7701522, 7701523, 7701524, 7701525 via cif-deposit CGI script. |
7701523.cif |
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Users of the data should acknowledge the original authors of the
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