Crystallography Open Database

Information card for entry 7702062

7702061 << 7702062 >> 7702063

Preview

Coordinates	7702062.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C46 H60 Cl6 N4 Ni4 O16
Calculated formula	C46 H60 Cl6 N4 Ni4 O16
Title of publication	Synthesis, magnetism and spectral studies of six defective dicubane tetranuclear {M4O6} (M = Ni(II), Co(II), Zn(II)) and three trinuclear Cd(II) complexes with polydentate Schiff base ligands.
Authors of publication	Jiang, Lin; Zhang, Dong-Yan; Suo, Jing-Jing; Gu, Wen; Tian, Jin-Lei; Liu, Xin; Yan, Shi-Ping
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2016
Journal volume	45
Journal issue	25
Pages of publication	10233 - 10248
a	9.4859 ± 0.0019 Å
b	19.986 ± 0.004 Å
c	14.498 ± 0.003 Å
α	90°
β	97.14 ± 0.03°
γ	90°
Cell volume	2727.3 ± 1 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1038
Residual factor for significantly intense reflections	0.0857
Weighted residual factors for significantly intense reflections	0.2325
Weighted residual factors for all reflections included in the refinement	0.2506
Goodness-of-fit parameter for all reflections included in the refinement	1.07
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
234724 (current)	2019-11-23	cif/ Adding structures of 7702061, 7702062, 7702063, 7702064, 7702065, 7702066, 7702067, 7702068, 7702069 via cif-deposit CGI script.	7702062.cif