Crystallography Open Database

Information card for entry 7702063

7702062 << 7702063 >> 7702064

Preview

Coordinates	7702063.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C44 H54 Br4 Co4 N4 O17
Calculated formula	C44 H54 Br4 Co4 N4 O17
Title of publication	Synthesis, magnetism and spectral studies of six defective dicubane tetranuclear {M4O6} (M = Ni(II), Co(II), Zn(II)) and three trinuclear Cd(II) complexes with polydentate Schiff base ligands.
Authors of publication	Jiang, Lin; Zhang, Dong-Yan; Suo, Jing-Jing; Gu, Wen; Tian, Jin-Lei; Liu, Xin; Yan, Shi-Ping
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2016
Journal volume	45
Journal issue	25
Pages of publication	10233 - 10248
a	17.1056 ± 0.0004 Å
b	11.7616 ± 0.0002 Å
c	27.3199 ± 0.0008 Å
α	90°
β	104.388 ± 0.002°
γ	90°
Cell volume	5324.1 ± 0.2 Å³
Cell temperature	125.4 ± 0.14 K
Ambient diffraction temperature	125.4 ± 0.14 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	I 1 2/c 1
Hall space group symbol	-I 2yc
Residual factor for all reflections	0.0396
Residual factor for significantly intense reflections	0.0318
Weighted residual factors for significantly intense reflections	0.0736
Weighted residual factors for all reflections included in the refinement	0.077
Goodness-of-fit parameter for all reflections included in the refinement	1.0662
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
234724 (current)	2019-11-23	cif/ Adding structures of 7702061, 7702062, 7702063, 7702064, 7702065, 7702066, 7702067, 7702068, 7702069 via cif-deposit CGI script.	7702063.cif