Crystallography Open Database

Information card for entry 7705891

Preview

Coordinates	7705891.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	Dy3 K5 Na5.34 Ni O139.78 Sb3 W30
Calculated formula	Dy3 K5 Na5.3333 Ni O139.773 Sb3 W30
Title of publication	Ionic strength effect on regulating the synthetic assembly of polyoxometalate clusters with slow magnetic relaxation behavior.
Authors of publication	Cai, Jing; Ye, Run; Liu, Xinhao; Guo, Leilei; Qiao, Xinrong
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	46
Pages of publication	16954 - 16961
a	18.2445 ± 0.0006 Å
b	19.9956 ± 0.0007 Å
c	24.4742 ± 0.0006 Å
α	93.078 ± 0.002°
β	99.426 ± 0.002°
γ	116.645 ± 0.003°
Cell volume	7790.2 ± 0.5 Å³
Cell temperature	186 ± 2 K
Ambient diffraction temperature	186 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1293
Residual factor for significantly intense reflections	0.0832
Weighted residual factors for significantly intense reflections	0.1928
Weighted residual factors for all reflections included in the refinement	0.2263
Goodness-of-fit parameter for all reflections included in the refinement	1.002
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
259698 (current)	2020-12-09	cif/ Adding structures of 7705891, 7705892, 7705893 via cif-deposit CGI script.	7705891.cif