Crystallography Open Database

Information card for entry 7705892

Preview

Coordinates	7705892.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	Ni0.21 O9.26 Sb0.21 W2.11
Calculated formula	Ni0.210526 O9.26316 Sb0.210526 W2.10526
Title of publication	Ionic strength effect on regulating the synthetic assembly of polyoxometalate clusters with slow magnetic relaxation behavior.
Authors of publication	Cai, Jing; Ye, Run; Liu, Xinhao; Guo, Leilei; Qiao, Xinrong
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	46
Pages of publication	16954 - 16961
a	17.8033 ± 0.0014 Å
b	18.5672 ± 0.0016 Å
c	14.166 ± 0.0012 Å
α	90°
β	113.239 ± 0.009°
γ	90°
Cell volume	4302.8 ± 0.7 Å³
Cell temperature	178.3 ± 0.6 K
Ambient diffraction temperature	178.3 ± 0.6 K
Number of distinct elements	4
Space group number	12
Hermann-Mauguin space group symbol	C 1 2/m 1
Hall space group symbol	-C 2y
Residual factor for all reflections	0.0814
Residual factor for significantly intense reflections	0.0678
Weighted residual factors for significantly intense reflections	0.1689
Weighted residual factors for all reflections included in the refinement	0.1788
Goodness-of-fit parameter for all reflections included in the refinement	1.088
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
259698 (current)	2020-12-09	cif/ Adding structures of 7705891, 7705892, 7705893 via cif-deposit CGI script.	7705892.cif