Crystallography Open Database

Information card for entry 7707499

Preview

Coordinates	7707499.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C87 H90 Al2 N4 S2
Calculated formula	C87 H90 Al2 N4 S2
Title of publication	Synthesis, characterization, and reactivity of group 13 hydride complexes based on amido-amine ligands.
Authors of publication	Dehmel, Maximilian; Köhler, Angelina; Görls, Helmar; Kretschmer, Robert
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	24
Pages of publication	8434 - 8445
a	14.5375 ± 0.0002 Å
b	16.7953 ± 0.0003 Å
c	20.1307 ± 0.0003 Å
α	104.701 ± 0.001°
β	99.954 ± 0.001°
γ	114.99 ± 0.001°
Cell volume	4083.37 ± 0.13 Å³
Cell temperature	133 ± 2 K
Ambient diffraction temperature	133 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.064
Residual factor for significantly intense reflections	0.0517
Weighted residual factors for significantly intense reflections	0.1414
Weighted residual factors for all reflections included in the refinement	0.1515
Goodness-of-fit parameter for all reflections included in the refinement	1.031
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
267144 (current)	2021-07-05	cif/ Updating files of 7707498, 7707499, 7707500, 7707501, 7707502, 7707503, 7707504, 7707505, 7707506, 7707507, 7707508, 7707509 Original log message: Adding full bibliography for 7707498--7707509.cif.	7707499.cif
265524	2021-05-27	cif/ Adding structures of 7707498, 7707499, 7707500, 7707501, 7707502, 7707503, 7707504, 7707505, 7707506, 7707507, 7707508, 7707509 via cif-deposit CGI script.	7707499.cif