Crystallography Open Database

Information card for entry 7707500

Preview

Coordinates	7707500.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H59 Al N2 Si3
Calculated formula	C28 H59 Al N2 Si3
SMILES	[Al]([Si](C)(C)C)([Si](C)(C)C)([Si](C)(C)C)[N]1(CCNc2c(cccc2C(C)C)C(C)C)CCCCC1
Title of publication	Synthesis, characterization, and reactivity of group 13 hydride complexes based on amido-amine ligands.
Authors of publication	Dehmel, Maximilian; Köhler, Angelina; Görls, Helmar; Kretschmer, Robert
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	24
Pages of publication	8434 - 8445
a	10.6055 ± 0.0003 Å
b	28.9712 ± 0.0006 Å
c	11.4037 ± 0.0002 Å
α	90°
β	96.681 ± 0.002°
γ	90°
Cell volume	3480.04 ± 0.14 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0428
Residual factor for significantly intense reflections	0.0342
Weighted residual factors for significantly intense reflections	0.0844
Weighted residual factors for all reflections included in the refinement	0.0899
Goodness-of-fit parameter for all reflections included in the refinement	1.036
Diffraction radiation wavelength	1.39222 Å
Diffraction radiation type	CuKβ
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
267144 (current)	2021-07-05	cif/ Updating files of 7707498, 7707499, 7707500, 7707501, 7707502, 7707503, 7707504, 7707505, 7707506, 7707507, 7707508, 7707509 Original log message: Adding full bibliography for 7707498--7707509.cif.	7707500.cif
265524	2021-05-27	cif/ Adding structures of 7707498, 7707499, 7707500, 7707501, 7707502, 7707503, 7707504, 7707505, 7707506, 7707507, 7707508, 7707509 via cif-deposit CGI script.	7707500.cif