Crystallography Open Database

Information card for entry 7707501

Preview

Coordinates	7707501.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C52 H55 Al N2
Calculated formula	C52 H55 Al N2
Title of publication	Synthesis, characterization, and reactivity of group 13 hydride complexes based on amido-amine ligands.
Authors of publication	Dehmel, Maximilian; Köhler, Angelina; Görls, Helmar; Kretschmer, Robert
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	24
Pages of publication	8434 - 8445
a	8.1677 ± 0.0002 Å
b	12.8522 ± 0.0004 Å
c	40.6365 ± 0.0016 Å
α	90°
β	90°
γ	90°
Cell volume	4265.7 ± 0.2 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	4
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0785
Residual factor for significantly intense reflections	0.0584
Weighted residual factors for significantly intense reflections	0.139
Weighted residual factors for all reflections included in the refinement	0.1578
Goodness-of-fit parameter for all reflections included in the refinement	1.039
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
267144 (current)	2021-07-05	cif/ Updating files of 7707498, 7707499, 7707500, 7707501, 7707502, 7707503, 7707504, 7707505, 7707506, 7707507, 7707508, 7707509 Original log message: Adding full bibliography for 7707498--7707509.cif.	7707501.cif
265524	2021-05-27	cif/ Adding structures of 7707498, 7707499, 7707500, 7707501, 7707502, 7707503, 7707504, 7707505, 7707506, 7707507, 7707508, 7707509 via cif-deposit CGI script.	7707501.cif