Crystallography Open Database

Information card for entry 7708916

Preview

Coordinates	7708916.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H66 As2 Cl2 Pd
Calculated formula	C36 H66 As2 Cl2 Pd
Title of publication	Tertiary arsine ligands for the Stille coupling reaction.
Authors of publication	Chishiro, Akane; Konishi, Masafumi; Inaba, Ryoto; Yumura, Takashi; Imoto, Hiroaki; Naka, Kensuke
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	51
Journal issue	1
Pages of publication	95 - 103
a	9.8187 ± 0.0006 Å
b	10.2351 ± 0.0007 Å
c	10.7679 ± 0.001 Å
α	112.662 ± 0.007°
β	107.773 ± 0.006°
γ	91.967 ± 0.005°
Cell volume	936.6 ± 0.14 Å³
Cell temperature	93.15 K
Ambient diffraction temperature	93.15 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0293
Residual factor for significantly intense reflections	0.0236
Weighted residual factors for significantly intense reflections	0.0531
Weighted residual factors for all reflections included in the refinement	0.0564
Goodness-of-fit parameter for all reflections included in the refinement	1.047
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
272648 (current)	2022-02-04	cif/ Updating files of 7708916, 7708917, 7708918, 7708919, 7708920 Original log message: Adding full bibliography for 7708916--7708920.cif.	7708916.cif
270869	2021-11-25	cif/ Adding structures of 7708916, 7708917, 7708918, 7708919, 7708920 via cif-deposit CGI script.	7708916.cif