Crystallography Open Database

Information card for entry 7708917

Preview

Coordinates	7708917.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C49 H20 As2 Cl4 F36 Pd
Calculated formula	C49 H20 As2 Cl4 F36 Pd
Title of publication	Tertiary arsine ligands for the Stille coupling reaction.
Authors of publication	Chishiro, Akane; Konishi, Masafumi; Inaba, Ryoto; Yumura, Takashi; Imoto, Hiroaki; Naka, Kensuke
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	51
Journal issue	1
Pages of publication	95 - 103
a	9.747 ± 0.004 Å
b	16.203 ± 0.006 Å
c	20.248 ± 0.008 Å
α	72.26 ± 0.016°
β	70.604 ± 0.012°
γ	73.957 ± 0.014°
Cell volume	2817.7 ± 1.9 Å³
Cell temperature	93.15 K
Ambient diffraction temperature	93.15 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0372
Residual factor for significantly intense reflections	0.0337
Weighted residual factors for significantly intense reflections	0.0802
Weighted residual factors for all reflections included in the refinement	0.0835
Goodness-of-fit parameter for all reflections included in the refinement	1.028
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
272648 (current)	2022-02-04	cif/ Updating files of 7708916, 7708917, 7708918, 7708919, 7708920 Original log message: Adding full bibliography for 7708916--7708920.cif.	7708917.cif
270869	2021-11-25	cif/ Adding structures of 7708916, 7708917, 7708918, 7708919, 7708920 via cif-deposit CGI script.	7708917.cif