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Information card for entry 7709940
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Coordinates | 7709940.cif |
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Original paper (by DOI) | HTML |
Formula | C24 H60 Al2 N6 |
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Calculated formula | C24 H60 Al2 N6 |
Title of publication | Synthesis and temperature-dependent NMR studies of monomeric and dimeric tris(dialkylamido)alanes |
Authors of publication | Schumann, Erik; Böhme, Uwe; Brendler, Erica; Mertens, Florian |
Journal of publication | Dalton Transactions |
Year of publication | 2022 |
a | 10.4271 ± 0.0004 Å |
b | 15.5764 ± 0.0006 Å |
c | 19.2818 ± 0.0007 Å |
α | 99.136 ± 0.003° |
β | 91.058 ± 0.003° |
γ | 96.911 ± 0.003° |
Cell volume | 3067.2 ± 0.2 Å3 |
Cell temperature | 153 ± 2 K |
Ambient diffraction temperature | 153 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0498 |
Residual factor for significantly intense reflections | 0.0374 |
Weighted residual factors for significantly intense reflections | 0.0912 |
Weighted residual factors for all reflections included in the refinement | 0.0999 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.057 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
Revision | Date | Message | Files |
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274419 (current) | 2022-04-08 | cif/ Adding structures of 7709940, 7709941 via cif-deposit CGI script. |
7709940.cif |
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Users of the data should acknowledge the original authors of the
structural data.