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Information card for entry 7709941
Preview
| Coordinates | 7709941.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C30 H66 Al2 N12 |
|---|---|
| Calculated formula | C30 H66 Al2 N12 |
| Title of publication | Synthesis and temperature-dependent NMR studies of monomeric and dimeric tris(dialkylamido)alanes |
| Authors of publication | Schumann, Erik; Böhme, Uwe; Brendler, Erica; Mertens, Florian |
| Journal of publication | Dalton Transactions |
| Year of publication | 2022 |
| a | 15.3937 ± 0.0005 Å |
| b | 15.3937 ± 0.0005 Å |
| c | 16.7614 ± 0.0005 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 3971.9 ± 0.2 Å3 |
| Cell temperature | 153 ± 2 K |
| Ambient diffraction temperature | 153 K |
| Number of distinct elements | 4 |
| Space group number | 86 |
| Hermann-Mauguin space group symbol | P 42/n :2 |
| Hall space group symbol | -P 4bc |
| Residual factor for all reflections | 0.0432 |
| Residual factor for significantly intense reflections | 0.0352 |
| Weighted residual factors for significantly intense reflections | 0.0889 |
| Weighted residual factors for all reflections included in the refinement | 0.0963 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.066 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 274419 (current) | 2022-04-08 | cif/ Adding structures of 7709940, 7709941 via cif-deposit CGI script. |
7709941.cif |
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Users of the data should acknowledge the original authors of the
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