Crystallography Open Database

Information card for entry 7710750

Preview

Coordinates	7710750.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	Magnesium bis(2-thiopyridyl)methylmethanide trimethylsiloxide
Formula	C30 H40 Mg2 N4 O2 S4 Si2
Calculated formula	C30 H40 Mg2 N4 O2 S4 Si2
Title of publication	Synthesis, Characterisation and Reactivity of Group 2 Complexes with a Thiopyridyl Scorpionate Ligand
Authors of publication	Stevens, Matthew Philip; Spray, Emily; Vitorica-Yrzebal, Inigo; Singh, Kuldip; Timmermann, Vanessa M.; Sotorrios, Lia; Macgregor, Stuart Alan; Ortu, Fabrizio
Journal of publication	Dalton Transactions
Year of publication	2022
a	13.12561 ± 0.00018 Å
b	9.98641 ± 0.00013 Å
c	13.71565 ± 0.00017 Å
α	90°
β	94.6324 ± 0.0012°
γ	90°
Cell volume	1791.94 ± 0.04 Å³
Cell temperature	100.03 ± 0.11 K
Ambient diffraction temperature	100.03 ± 0.11 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0334
Residual factor for significantly intense reflections	0.0309
Weighted residual factors for significantly intense reflections	0.0811
Weighted residual factors for all reflections included in the refinement	0.0825
Goodness-of-fit parameter for all reflections included in the refinement	1.057
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
276839 (current)	2022-07-23	cif/ Adding structures of 7710749, 7710750, 7710751, 7710752, 7710753, 7710754, 7710755, 7710756 via cif-deposit CGI script.	7710750.cif