Crystallography Open Database

Information card for entry 7711933

7711932 << 7711933 >> 7711934

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Coordinates	7711933.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	[{κP,κC-(i-Pr)2PO-C6H4}{NH2OBn}Ni(Cl/Br)]
Formula	C19 H27 Br0.26 Cl0.74 N Ni O2 P
Calculated formula	C19 H27 Br0.2655 Cl0.7345 N Ni O2 P
Title of publication	Reactivities of cyclonickellated complexes with hydroxylamines: formation of κ<sup>O</sup>-hydroxylamine and κ<sup>N</sup>-imine adducts and a κ<sup>O</sup>, κ<sup>N</sup>-aminoxide derivative.
Authors of publication	Sarker, Rajib K.; Mangin, Loïc P; Zargarian, Davit
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2023
Journal volume	52
Journal issue	2
Pages of publication	366 - 375
a	9.2167 ± 0.0003 Å
b	10.7893 ± 0.0003 Å
c	11.1469 ± 0.0003 Å
α	108.309 ± 0.001°
β	99.259 ± 0.001°
γ	99.244 ± 0.001°
Cell volume	1011.92 ± 0.05 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0237
Residual factor for significantly intense reflections	0.0236
Weighted residual factors for significantly intense reflections	0.0639
Weighted residual factors for all reflections included in the refinement	0.064
Goodness-of-fit parameter for all reflections included in the refinement	1.063
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
283290 (current)	2023-05-05	cif/ Updating files of 7711929, 7711930, 7711931, 7711932, 7711933, 7711934, 7711935, 7711936, 7711937, 7711938, 7711939 Original log message: Adding full bibliography for 7711929--7711939.cif.	7711933.cif
279895	2022-12-15	cif/ Adding structures of 7711929, 7711930, 7711931, 7711932, 7711933, 7711934, 7711935, 7711936, 7711937, 7711938, 7711939 via cif-deposit CGI script.	7711933.cif