Crystallography Open Database

Information card for entry 7714466

Preview

Coordinates	7714466.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	1
Formula	C1.71 F3.43 Ge0.14 O0.57
Calculated formula	C1.71429 F3.42857 Ge0.142857 O0.571429
Title of publication	A neutral germanium-centred hard and soft lewis superacid and its unique reactivity towards hydrosilanes.
Authors of publication	Tschernuth, Florian S.; Kostenko, Arseni; Stigler, Sebastian; Gradenegger, Anna; Inoue, Shigeyoshi
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2023
Journal volume	53
Journal issue	1
Pages of publication	74 - 81
a	18.7356 ± 0.0009 Å
b	18.5219 ± 0.001 Å
c	11.6384 ± 0.0006 Å
α	90°
β	90°
γ	90°
Cell volume	4038.7 ± 0.4 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	4
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0892
Residual factor for significantly intense reflections	0.084
Weighted residual factors for significantly intense reflections	0.2274
Weighted residual factors for all reflections included in the refinement	0.2352
Goodness-of-fit parameter for all reflections included in the refinement	1.049
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
289462 (current)	2024-02-04	cif/ Updating files of 7714462, 7714463, 7714464, 7714465, 7714466 Original log message: Adding full bibliography for 7714462--7714466.cif.	7714466.cif
287629	2023-11-16	cif/ Adding structures of 7714462, 7714463, 7714464, 7714465, 7714466 via cif-deposit CGI script.	7714466.cif