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Information card for entry 7714550
Preview
| Coordinates | 7714550.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C68 H100 Gd2 N6 O2 Si2 |
|---|---|
| Calculated formula | C68 H100 Gd2 N6 O2 Si2 |
| Title of publication | Synthesis and catalytic activity of tetradentate β-diketiminato rare-earth metal monoalkyl complexes in tandem Oppenauer oxidation and cross-aldol condensation. |
| Authors of publication | Zou, Haiyan; Wang, Ziqian; Guo, Dianjun; Zhang, Lijun; Wang, Shaowu; Zhu, Xiancui |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2023 |
| Journal volume | 53 |
| Journal issue | 1 |
| Pages of publication | 267 - 275 |
| a | 35.524 ± 0.003 Å |
| b | 22.8423 ± 0.0016 Å |
| c | 23.6243 ± 0.0016 Å |
| α | 90° |
| β | 129.856 ± 0.001° |
| γ | 90° |
| Cell volume | 14715.9 ± 1.9 Å3 |
| Cell temperature | 293.15 K |
| Ambient diffraction temperature | 293.15 K |
| Number of distinct elements | 6 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.0811 |
| Residual factor for significantly intense reflections | 0.0394 |
| Weighted residual factors for significantly intense reflections | 0.0774 |
| Weighted residual factors for all reflections included in the refinement | 0.0891 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.013 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 289467 (current) | 2024-02-04 | cif/ Updating files of 7714545, 7714546, 7714547, 7714548, 7714549, 7714550, 7714551, 7714552 Original log message: Adding full bibliography for 7714545--7714552.cif. |
7714550.cif |
| 287794 | 2023-11-25 | cif/ Adding structures of 7714545, 7714546, 7714547, 7714548, 7714549, 7714550, 7714551, 7714552 via cif-deposit CGI script. |
7714550.cif |
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Users of the data should acknowledge the original authors of the
structural data.