Crystallography Open Database

Information card for entry 7714551

Preview

Coordinates	7714551.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C68 H100 N6 O2 Si2 Yb2
Calculated formula	C68 H100 N6 O2 Si2 Yb2
Title of publication	Synthesis and catalytic activity of tetradentate β-diketiminato rare-earth metal monoalkyl complexes in tandem Oppenauer oxidation and cross-aldol condensation.
Authors of publication	Zou, Haiyan; Wang, Ziqian; Guo, Dianjun; Zhang, Lijun; Wang, Shaowu; Zhu, Xiancui
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2023
Journal volume	53
Journal issue	1
Pages of publication	267 - 275
a	35.46 ± 0.05 Å
b	23.07 ± 0.03 Å
c	23.6 ± 0.03 Å
α	90°
β	129.797 ± 0.013°
γ	90°
Cell volume	14833 ± 3 Å³
Cell temperature	293.15 K
Ambient diffraction temperature	293.15 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0875
Residual factor for significantly intense reflections	0.0435
Weighted residual factors for significantly intense reflections	0.1007
Weighted residual factors for all reflections included in the refinement	0.1158
Goodness-of-fit parameter for all reflections included in the refinement	1.029
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
289467 (current)	2024-02-04	cif/ Updating files of 7714545, 7714546, 7714547, 7714548, 7714549, 7714550, 7714551, 7714552 Original log message: Adding full bibliography for 7714545--7714552.cif.	7714551.cif
287794	2023-11-25	cif/ Adding structures of 7714545, 7714546, 7714547, 7714548, 7714549, 7714550, 7714551, 7714552 via cif-deposit CGI script.	7714551.cif